Flash spark plasma sintering of zirconia nanoparticles: Electro-thermal-mechanical-microstructural simulation and scalability solutions

نویسندگان

چکیده

Flash sintering is a very promising method with great potential for the ultra-rapid production of objects firing processes mere seconds. However, transition from few millimeters samples to larger scales key issue. In this study, we explore spark plasma approach allowing stable hybrid heating in flash condition and producing near net shape sintered specimens. Two electric current configurations are employed diameters 15 30 mm determine effect scale change concentration. These experiments coupled Multiphysics simulation indicate that conditions can be reached even if electrical concentration effective at small sizes, it generates peripheral hot spots large specimen dimensions. The blackening on zirconia specimens acts then as an indicator thermal history.

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ژورنال

عنوان ژورنال: Journal of The European Ceramic Society

سال: 2022

ISSN: ['0955-2219', '1873-619X']

DOI: https://doi.org/10.1016/j.jeurceramsoc.2021.09.021